Multidimensional HPLC of Polymers
Springer Science & Business Media, Jun 12, 2013 - Technology & Engineering - 280 pages
This book presents the principle ideas of combining different analytical techniques in multi-dimensional analysis schemes. It reviews the basic principles and instrumentation of multi-dimensional chromatography and the hyphenation of liquid chromatography with selective spectroscopic detectors and presents experimental protocols for the analysis of complex polymers.
It is the consequent continuation of "HPLC of Polymers" from 1999 by the same authors. Like its 'predecessor', this book discusses the theoretical background, equipment, experimental procedures and applications for each separation technique, but in contrast treats multi-dimensional and coupled techniques. "Multidimensional HPLC of Polymers" intends to review the state of the art in polymer chromatography and to summarize the developments in the field during the last 15 years. With its tutorial and laboratory manual style it is written for beginners as well as for experienced chromatographers, and will enable its readers (polymer chemists, physicists and material scientists, as well as students of polymer and analytical sciences) to optimize the experimental conditions for their specific separation problems.
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adsorption American Chemical Society Anal Chem analysis analyzed behaviour blend block copolymers branched Business Media calibration curve Calibration Standards chemical composition Chromatogr Chromatographic System Column Temperature complex polymers components concentration contour plot coupled critical conditions detection determined ELSD eluent Elution Volume mL endgroups EPDM exclusion chromatography ﬁrst dimension ﬂow rate FTIR functionality fractions g/mol gradient HPLC graft copolymer heterogeneity homopolymers HPLC interaction chromatography LCCC light scattering detector linear liquid chromatography Macko Macromolecules MALDI-TOF methacrylate methods methyl mL/min mobile phase mode molar mass distribution molecular molecules monomer Nucleosil obtained oligomer parameter Pasch H PDMS permission of Springer PMMA polymer polymer chain polymerization polyoleﬁns polystyrene pore Provder repeat units reprinted retention sample SEC separation second dimension separation according size exclusion chromatography solvent speciﬁc spectra Springer Science star polymers stationary phase styrene sufﬁcient techniques Trathnigg typical viscosity