Multidimensional HPLC of Polymers

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Springer Science & Business Media, Jun 12, 2013 - Technology & Engineering - 280 pages
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This book presents the principle ideas of combining different analytical techniques in multi-dimensional analysis schemes. It reviews the basic principles and instrumentation of multi-dimensional chromatography and the hyphenation of liquid chromatography with selective spectroscopic detectors and presents experimental protocols for the analysis of complex polymers.
It is the consequent continuation of "HPLC of Polymers" from 1999 by the same authors. Like its 'predecessor', this book discusses the theoretical background, equipment, experimental procedures and applications for each separation technique, but in contrast treats multi-dimensional and coupled techniques. "Multidimensional HPLC of Polymers" intends to review the state of the art in polymer chromatography and to summarize the developments in the field during the last 15 years. With its tutorial and laboratory manual style it is written for beginners as well as for experienced chromatographers, and will enable its readers (polymer chemists, physicists and material scientists, as well as students of polymer and analytical sciences) to optimize the experimental conditions for their specific separation problems.
 

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Contents

Introduction
1
Theory of Polymer Chromatography
17
Interactive Modes of Polymer Chromatography
27
Equipment and Materials
36
Multidetector Size Exclusion Chromatography
55
TwoDimensional Liquid Chromatography
94
Hyphenation of Polymer Chromatography with InformationRich Detectors
183
Polyolefin Analysis by Multidimensional Liquid Chromatography
247
Conclusions and Future Trends
272
Index
277
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